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  • It is preferred that the reaction is run at temperatures ranging from 40??? to -40??? C., with the preferred temperature ranging from -25??? C. to +25??? C. It is preferred that the reaction be run in the presence of a drying agent, such as magnesium sulfate, sodium sulfate or molecular sieves of 2 ???-8 ???, with the most preferred molecular sieves being molecular sieves of 3-5 ??? and especially
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