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  • Step (b) is suitably carried out at a temperature from about 100??? C. to about 300??? C., preferably at a temperature of from about 120??? C. to about 200??? C., and more preferably at about 150??? C. to about 175??? C. The temperature to be employed is mainly determined by such factors as activity of the catalytic system and the desired reaction time It is preferably to operate at the minimum te
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