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  • A process for preparing a bulk monocrystalline gallium-containing nitride in an autoclave according to claim 24, wherein said ions of alkali metals are introduced in the form of mineralizers selected from alkali metals and compounds thereof, such as azides, nitrides, amides, amido-imides, imides, and/or hydrides, for forming an ammono-basic supercritical ammonia solution, which does not contain io
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