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  • The ethyl acetate started to condense at 130??? C., and was considerably distilled off after 15 minutes at 150??? C. The crude TKAS reaction product had the form of wax-like spherulites, which dissolved in organic solvents such as petroleum ether, cyclohexane, ethyl acetate, dichloroethane, carbon tetrachloride, acetone, and chlorobenzene.
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