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  • From the foregoing dehydration, a lower alkylene-1,ldiphosphonate salt is formed and such can be readily converted to the free acid by dissolving or suspending the salt in water and passing through a strongly acidic cation exchange resin bed or adding an acid, particularly a strong mineral acid (H SO HCl, H PO and the like) to precipitate from the solution a salt of the acid, for example, adding H
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