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  • The reaction is allowed to proceed for from about 15 minutes to about 6 hours, depending on the reactants, the solvent, the concentrations, and other factors, such as the temperature which can be from about 0??? C. to about 60??? C., conveniently at about room temperature, i.e. 25??? C. The formula 1 product can be isolated from the reaction mixture by any appropriate techniques such as by chromat
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