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  • The aqueous acidic phase was then treated with 40% NaOH with cooling, extracted with ether (and worked up by washing with water, with brine and drying with an anhydrous drying agent such as magnesium sulfate or sodium sulfate before evaporation???this work up procedure is referred to as work up in the usual manner hereinafter) to give 144.7 g of a sludge.
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