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  • The reduction of the esters of formula (IIIB) can be achieved using diisobutylaluminium hydride (DIBAL) in a suitable solvent at a temperature of less than 0??? C., preferably less than ???60??? C. Suitable solvents include hydrocarbons such as pentane, hexane and toluene, ethers such as tetrahydrofuran, and mixtures thereof.
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